Formation of α-TeO2 pearl-like microwires templated on porous microtubes through thermal oxidation of Te microtubes
| Autor: | M. Siciliano, T. Siciliano, M. Tepore, Alessandra Genga, Emanuela Filippo, G. Micocci |
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| Přispěvatelé: | Filippo, Emanuela, Siciliano, Tiziana, Genga, Alessandra, Micocci, Gioacchino, Siciliano, Maria, Tepore, Marco |
| Rok vydání: | 2013 |
| Předmět: |
Thermal oxidation
Materials science microtubes Scanning electron microscope General Physics and Astronomy Nanotechnology Surfaces and Interfaces General Chemistry Condensed Matter Physics Microstructure Surfaces Coatings and Films law.invention symbols.namesake Chemical engineering law Transmission electron microscopy Microscopy symbols Electron microscope Porous medium Raman spectroscopy |
| Zdroj: | Applied Surface Science. 265:329-333 |
| ISSN: | 0169-4332 |
| DOI: | 10.1016/j.apsusc.2012.11.005 |
| Popis: | The current work demonstrates the first reported successful synthesis of unique alpha-TeO2 hybrid microstructures through thermal oxidation of Te microtubes in a horizontal tube furnace at different temperatures in the range 220-470 degrees C, under oxygen flow. The obtained microstructures were carefully characterized by scanning electron microscopy, transmission electron microscopy, X-ray diffraction and Raman spectroscopy. They exhibited characteristic morphologies with porous scaffold microtubes covered along their whole length with pearl-like microwires. The possible formation mechanism of the obtained microstructures was also discussed. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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