Versailles Project on Advanced Materials and Standards interlaboratory study on intensity calibration for x-ray photoelectron spectroscopy instruments using low-density polyethylene

Autor: Reed, Benjamen, Cant, David, Spencer, Steve, Carmona-Carmona, Abraham Jorge, Bushell, Adam, Herrera-Gómez, Alberto, Kurokawa, Akira, Thissen, Andreas, Thomas, Andrew, Britton, Andrew, Bernasik, Andrzej, Fuchs, Anne, Baddorf, Arthur, Bock, Bernd, Theilacker, Bill, Cheng, Bin, Castner, David, Morgan, David, Valley, David, Willneff, Elizabeth, Smith, Emily, Nolot, Emmanuel, Xie, Fangyan, Zorn, Gilad, Smith, Graham, Yasufuku, Hideyuki, Fenton, Jeffery, Chen, Jian, Counsell, Jonathan, Radnik, Jörg, Gaskell, Karen, Artyushkova, Kateryna, Yang, Li, Zhang, Lulu, Eguchi, Makiho, Walker, Marc, Hajdyła, Mariusz, Marzec, Mateusz, Linford, Matthew, Kubota, Naoyoshi, Cortazar-Martínez, Orlando, Dietrich, Paul, Satoh, Riki, Schroeder, Sven, Avval, Tahereh, Nagatomi, Takaharu, Fernandez, Vincent, Lake, Wayne, Azuma, Yasushi, Yoshikawa, Yusuke, Compean-Gonzalez, Claudia L., Ceccone, Giacomo, Shard, Alexander G.
Přispěvatelé: National Physical Laboratory [Teddington] (NPL), Centro de Investigacion y de Estudios Avanzados del Instituto Politécnico Nacional (CINVESTAV), Thermo Fisher Scientific (Bremen) GmbH, National Metrology Institute of Japan, National Institute od Advanced Industrial Science and Technology, SPECS Surface Nano Analysis GmbH, University of Manchester [Manchester], University of Leeds, AGH University of Science and Technology [Krakow, PL] (AGH UST), Robert Bosch Gmbh [Schwieberdingen], Oak Ridge National Laboratory [Oak Ridge] (ORNL), UT-Battelle, LLC, Tascon GmbH, Medtronic SNT, Medtronic, Beijing University of Chemical Technology, University of Washington [Seattle], Cardiff University, Phys Elect Inc, University of Nottingham, UK (UON), Commissariat à l'énergie atomique et aux énergies alternatives - Laboratoire d'Electronique et de Technologie de l'Information (CEA-LETI), Direction de Recherche Technologique (CEA) (DRT (CEA)), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA), National Sun Yat-Sen University (NSYSU), GE Res, University of Chester, National Institute for Materials Science (NIMS), Kratos Analyt Ltd, BAM Bundesanstalt für Materialforschung u. -prüfung, University of Maryland [Baltimore], Xi'an Jiaotong-Liverpool University [Suzhou], Nippon Steel Technol Co Ltd, University of Warwick [Coventry], Brigham Young University (BYU), Asahi Kasei Corp, Institut des Matériaux Jean Rouxel (IMN), Université de Nantes - UFR des Sciences et des Techniques (UN UFR ST), Université de Nantes (UN)-Université de Nantes (UN)-Ecole Polytechnique de l'Université de Nantes (EPUN), Université de Nantes (UN)-Université de Nantes (UN)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS), AWE, Yazaki Corp, European Commission - Joint Research Centre [Ispra] (JRC), Université de Nantes (UN)-Université de Nantes (UN)-Centre National de la Recherche Scientifique (CNRS)-Institut de Chimie du CNRS (INC)-Ecole Polytechnique de l'Université de Nantes (EPUN), Université de Nantes (UN)-Université de Nantes (UN)
Jazyk: angličtina
Rok vydání: 2020
Předmět:
Zdroj: Journal of Vacuum Science & Technology A
Journal of Vacuum Science & Technology A, 2020, 38 (6), pp.063208. ⟨10.1116/6.0000577⟩
Journal of Vacuum Science and Technology A
Journal of Vacuum Science and Technology A, American Vacuum Society, 2020, 38 (6), pp.063208. ⟨10.1116/6.0000577⟩
J Vac Sci Technol A
NPL Versailles project 2020, ' Versailles Project on Advanced Materials and Standards interlaboratory study on intensity calibration for x-ray photoelectron spectroscopy instruments using low-density polyethylene ', Journal of Vacuum Science & Technology A . https://doi.org/10.1116/6.0000577
ISSN: 0734-2101
Popis: International audience; We report the results of a Versailles Project on Advanced Materials and Standards interlaboratory study on the intensity scale calibration of x-ray photoelectron spectrometers using low-density polyethylene (LDPE) as an alternative material to gold, silver, and copper. An improved set of LDPE reference spectra, corrected for different instrument geometries using a quartz-monochromated Al Kα x-ray source, was developed using data provided by participants in this study. Using these new reference spectra, a transmission function was calculated for each dataset that participants provided. When compared to a similar calibration procedure using the NPL reference spectra for gold, the LDPE intensity calibration method achieves an absolute offset of ∼3.0% and a systematic deviation of ±6.5% on average across all participants. For spectra recorded at high pass energies (≥90 eV), values of absolute offset and systematic deviation are ∼5.8% and ±5.7%, respectively, whereas for spectra collected at lower pass energies (
Databáze: OpenAIRE