[Method-performance studies of notified analytical method for clofentezine]

Autor: Munetomo Nakamura, Osamu Utsunomiya, Kaoru Takahata, Takashi Tatsuno, Yasuaki Kondo, Masatake Toyoda, Harumi Osada, Kumiko Sasaki, Tsuyoshi Imazawa
Rok vydání: 2002
Předmět:
Zdroj: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan. 42(4)
ISSN: 0015-6426
Popis: Method-performance studies were conducted for the notified revised analytical method of clofentezine. Clofentezine spiked in azuki beans, apple, orange, banana, grape, tea powder and tea extract at the level of 0.2 microgram/g (2 micrograms/g for tea) was analyzed in replicate in 6 laboratories. Mean values of recovery from 7 crops ranged from 78.4 to 85.2%. Repeatability relative standard deviation values ranged from 2.2 to 4.6% and reproducibility standard deviation values ranged from 4.8 to 10.3%. The detection limits were 0.005-0.01 microgram/g. These results show the notified analytical method has good performance.
Databáze: OpenAIRE