Nanoscale control of high-quality boron-doped ultrananodiamond on dioxide titanium nanotubes as a porous composite
| Autor: | L.G. Vernasqui, Silvia Sizuka Oishi, Andre F. Sardinha, N.G. Ferreira |
|---|---|
| Rok vydání: | 2021 |
| Předmět: |
Materials science
Scanning electron microscope chemistry.chemical_element Composite Nanoporous material 02 engineering and technology Chemical vapor deposition Substrate (electronics) engineering.material 01 natural sciences Biomaterials symbols.namesake 0103 physical sciences Boron Titanium 010302 applied physics Mining engineering. Metallurgy Argon Anodizing TN1-997 Metals and Alloys Diamond 021001 nanoscience & nanotechnology Surfaces Coatings and Films Dioxide titanium nanotubes chemistry Chemical engineering Ultrananocrystalline boron-doped diamond Ceramics and Composites symbols engineering Process control 0210 nano-technology Raman spectroscopy |
| Zdroj: | Journal of Materials Research and Technology, Vol 12, Iss, Pp 597-612 (2021) |
| ISSN: | 2238-7854 |
| DOI: | 10.1016/j.jmrt.2021.02.099 |
| Popis: | A synthesis from micro to ultrananocrystalline boron-doped diamond (BDD/B-UNCD) requires a substrate pre-treatment by different seeding processes. Besides, for chemical vapor deposition, porous films demand high controlled two-step processes not only related to the substrate seeding but also to the suitable gas phase balancing among hydrogen, methane, boron, and argon. Firstly, systematic control of dioxide titanium nanotubes (DTNT) anodization parameters was performed including the thermally treated samples not to mention their photoelectrochemical response. Thus, high-quality porous B-UNCD was successfully obtained on DTNT substrate keeping its morphology by choosing the appropriated DTNT anodization as well as the B-UNCD growth parameters. Moreover, both B-UNCD/DTNT/Ti and DTNT were analyzed by field emission gun - scanning electron microscopy, Raman spectroscopy, X-ray diffraction, and photoelectrochemical response measurements. The results confirmed their quality and properties as well as their nanoscale control. |
| Databáze: | OpenAIRE |
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