Surface characterization of different surface treatments associations with plasma and bonding analysis of Y-TZP and the veneering ceramic

Autor: Sandro Basso Bitencourt, Estevam A. Bonfante, Elidiane Cipriano Rangel, Natália Almeida Bastos-Bitencourt, Nilson Cristino da Cruz, Grace M. De Souza, Daniela Micheline dos Santos, Aldiéris Alves Pesqueira
Přispěvatelé: Universidade Estadual Paulista (UNESP), Universidade de São Paulo (USP), University of Toronto
Jazyk: angličtina
Rok vydání: 2021
Předmět:
Zdroj: Scopus
Repositório Institucional da UNESP
Universidade Estadual Paulista (UNESP)
instacron:UNESP
Repositório Institucional da USP (Biblioteca Digital da Produção Intelectual)
Universidade de São Paulo (USP)
instacron:USP
Popis: Made available in DSpace on 2022-04-29T08:35:44Z (GMT). No. of bitstreams: 0 Previous issue date: 2021-01-01 Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq) Objectives: To characterize the surface of zirconia (Y-TZP) submitted to different surface treatments (with and without plasma associations) and to evaluate the shear bond strength (SBS) between veneering ceramic (VC) and Y-TZP after different aging methods. Methods: 301 Y-TZP specimens were fabricated and distributed into 7 groups: C (control): no treatment; Al: airborne abrasion with 27 μm Al2O3 particle; L: liner; P: plasma; Al + L: airborne + liner; Al + P: airborne + plasma; P + L: plasma + liner. The Y-TZP surface was characterized by SEM, EDS, AFM, surface profilometry, surface-free energy (SFE), and XRD. SBS between Y-TZP and VC was verified after three aging protocols: initial, after hydrothermal aging (autoclave for 5 h), or thermal fatigue (30,000 baths – 5–55 °C). One- (profilometry, SFE) and two-way ANOVA (SBS), and Tukey's HSD test were used. Results: For the plasma groups, a full globular surface coverage was observed (SEM, AFM). Si was found for Al, L, Al + L, and P + L. Roughness was lower for C, P, and Al + P. For SFE, the highest values were found when the liner was applied (>74.59 nm/Nm). The highest monoclinic content was observed for Al + L (6.96%) and Al + P (5.86%). For the initial period, Al and P + L presented the lowest SBS values ( 0.331). The highest SBS values were found for L, P, and P + L (hydrothermal aging) and for P, L, Al + L, and Al + P (thermal fatigue). Significance: Changes in Y-TZP topography and the SBS with the VC were found, according to treatments performed. Plasma treatment improved SBS and did not cause phase transformation. Department of Dental Materials and Prosthodontics Aracatuba School of Dentistry Sao Paulo State University (UNESP) Department of Operative Dentistry Endodontics and Dental Materials Bauru School of Dentistry University of São Paulo, Bauru Laboratory of Technological Plasmas (LaPTec) Engineering College Sao Paulo State University (UNESP), Sorocaba Department of Prosthodontics and Periodontology Bauru School of Dentistry University of São Paulo, Bauru Faculty of Dentistry University of Toronto Department of Dental Materials and Prosthodontics Aracatuba School of Dentistry Sao Paulo State University (UNESP) Laboratory of Technological Plasmas (LaPTec) Engineering College Sao Paulo State University (UNESP), Sorocaba FAPESP: 2012/19078-7 FAPESP: 2015/11412-3 FAPESP: 2017/13933-6 FAPESP: 2018/24984-3 CNPq: 304589/2017-9 CNPq: 426719/2018-2 CNPq: 434487/2018-0 FAPESP: EMU 2016/18818-8
Databáze: OpenAIRE