Raman microprobe technique diagnostic of YBCO films produced by laser ablation
Autor: | S. Pestelli, Maria Allegrini, M. Zoppi, P Martini, Francesco Fuso, Ennio Arimondo, A Diodati, Marina Mazzoni, L. Ulivi |
---|---|
Rok vydání: | 1994 |
Předmět: | |
Zdroj: | Il Nuovo Cimento D. 16:2011-2017 |
ISSN: | 1826-9893 0392-6737 |
DOI: | 10.1007/bf02471860 |
Popis: | We have used a Raman microprobe technique for the characterisation and the diagnostic of YBCO superconducting thin films deposited by Pulsed-Laser Ablation (PLA) on MgO insulating substrates. Using polarisation analysis associated with sample rotations we developed a method for films orientation determination without any request for absolute calibration of the Raman spectra. The use of a bidimensional multichannel detector (OMA 4) allowed an overall detection time of 40 minutes. Each spectrum (shift range from 100 cm−1 to 700 cm−1) takes about 600 seconds. The results of this detection were used to determine the oxygen content, from the position of the Raman mode at 500 cm−1 Homogeneity was checked with the spatial resolution allowed by the dimension of the focused laser beam (10 μm). |
Databáze: | OpenAIRE |
Externí odkaz: |