'Pure by NMR'?
| Autor: | Edward D. Savory, Angela J. Russell, Timothy D. W. Claridge, Andrew D. Smith, Stephen G. Davies, Paul M. Roberts, Mario E. C. Polywka |
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| Jazyk: | angličtina |
| Rok vydání: | 2008 |
| Předmět: | |
| Zdroj: | Organic letters. 10(23) |
| ISSN: | 1523-7052 1523-7060 |
| Popis: | Integration of a (13)C-(1)H satellite peak of a given (12)C-(1)H parent resonance within a quantitative (1)H NMR spectrum and comparison to the minor component represents a simple protocol for the accurate determination of diastereoisomeric ratios of up to 1000:1 (i.e., 99.8% de). |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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