Method validation and dissipation kinetics of the new HPPD inhibitor QYR301 in rice, paddy water and paddy soil using a QuEChERS-based method and LC-MS/MS
| Autor: | Wenlei Guo, Jinxin Wang, Xiaolin Zhang, Weitang Liu, Penglei Sun, Lipeng Wang, Feng Bei, Hengzhi Wang |
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| Rok vydání: | 2019 |
| Předmět: |
Health
Toxicology and Mutagenesis Kinetics 0211 other engineering and technologies 02 engineering and technology 010501 environmental sciences Mass spectrometry Quechers 01 natural sciences Tandem Mass Spectrometry Lc ms ms Soil Pollutants Sample preparation 0105 earth and related environmental sciences 021110 strategic defence & security studies Chromatography Chemistry Herbicides Public Health Environmental and Occupational Health food and beverages Esters Oryza General Medicine Straw Pollution Paddy field Pyrazoles Brown rice Water Pollutants Chemical Chromatography Liquid Environmental Monitoring Half-Life |
| Zdroj: | Ecotoxicology and environmental safety. 184 |
| ISSN: | 1090-2414 |
| Popis: | A rapid and simple method based on liquid chromatography-tandem mass spectrometry (LC-MS/MS) of sample preparation using QuEChERS was developed for detecting residues of QYR301, a new HPPD-inhibiting herbicide, in rice plant (straw), water, soil, rice hull and brown rice (BR). To eliminate matrix interference, matrix-matched calibrations with satisfactory linearity (R2 > 0.99) were used for accurate quantification. The method showed recoveries of 90.3–108.1% and relative standard deviations (RSDs) |
| Databáze: | OpenAIRE |
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