Validation and estimation of uncertainty of an LC-MS/MS method for the simultaneous determination of 34 mycotoxins in cocoa beans

Autor:	Daiane Cássia Pereira, Abreu, Eugenia Azevedo, Vargas, Fabiano Aurélio, da Silva Oliveira, Fernando Diniz, Madureira, Mateus Batista, Gomes, Matheus Julien Ferreira, Bazzana, Adelir Aparecida, Saczk
Rok vydání:	2023
Předmět:	Cacao Tandem Mass Spectrometry Uncertainty General Medicine Mycotoxins Chromatography High Pressure Liquid Chromatography Liquid Food Science Analytical Chemistry
Zdroj:	Food Chemistry. 399:133902
ISSN:	0308-8146
DOI:	10.1016/j.foodchem.2022.133902
Popis:	The aim of this manuscript was to validate and apply an analytical methodology for the simultaneous determination of 34 mycotoxins in cocoa. The extraction method used in the tests was a liquid-liquid partition by NaCl addition with a freezing step followed by quantification using LC-MS/MS. The results were discussed based on national and international directives for food contaminants. The recoveries and precision were adequate, except for the mycotoxins ionized with the ammonium adduct (NH
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::6ce8f84945c9e64d45e0572659e035d4 https://doi.org/10.1016/j.foodchem.2022.133902 Zobrazit plný text záznamu Full Text from ScienceDirect