Apparent anisotropy of adhesive bonds with weak adhesion and non-destructive evaluation of interfacial properties

Autor: Jocelyne Galy, Michel Castaings, Mathieu Renier, Emmanuel Siryabe, Anissa Meziane
Přispěvatelé: Institut de Mécanique et d'Ingénierie de Bordeaux (I2M), Institut National de la Recherche Agronomique (INRA)-Université de Bordeaux (UB)-École Nationale Supérieure d'Arts et Métiers (ENSAM), Arts et Métiers Sciences et Technologies, HESAM Université (HESAM)-HESAM Université (HESAM)-Arts et Métiers Sciences et Technologies, HESAM Université (HESAM)-HESAM Université (HESAM)-Institut Polytechnique de Bordeaux-Centre National de la Recherche Scientifique (CNRS), Institut Jean Le Rond d'Alembert (DALEMBERT), Université Pierre et Marie Curie - Paris 6 (UPMC)-Centre National de la Recherche Scientifique (CNRS), Ingénierie des Matériaux Polymères (IMP), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National des Sciences Appliquées de Lyon (INSA Lyon), Université de Lyon-Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA)-Université Jean Monnet [Saint-Étienne] (UJM)-Centre National de la Recherche Scientifique (CNRS), Laboratoire de Mécanique Physique (LMP), Université Sciences et Technologies - Bordeaux 1-Centre National de la Recherche Scientifique (CNRS), HESAM Université - Communauté d'universités et d'établissements Hautes écoles Sorbonne Arts et métiers université (HESAM)-HESAM Université - Communauté d'universités et d'établissements Hautes écoles Sorbonne Arts et métiers université (HESAM)-Arts et Métiers Sciences et Technologies, HESAM Université - Communauté d'universités et d'établissements Hautes écoles Sorbonne Arts et métiers université (HESAM)-HESAM Université - Communauté d'universités et d'établissements Hautes écoles Sorbonne Arts et métiers université (HESAM)-Institut Polytechnique de Bordeaux-Centre National de la Recherche Scientifique (CNRS), Institut Jean le Rond d'Alembert (DALEMBERT), Université de Lyon-Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA)-Université Jean Monnet - Saint-Étienne (UJM)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS), Université Sciences et Technologies - Bordeaux 1 (UB)-Centre National de la Recherche Scientifique (CNRS), Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS)-Université Jean Monnet [Saint-Étienne] (UJM)-Institut National des Sciences Appliquées de Lyon (INSA Lyon), Université de Lyon-Institut National des Sciences Appliquées (INSA)-Université de Lyon-Institut National des Sciences Appliquées (INSA)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon, Centre National de la Recherche Scientifique (CNRS)-Université Sciences et Technologies - Bordeaux 1
Rok vydání: 2017
Předmět:
Zdroj: Ultrasonics
Ultrasonics, Elsevier, 2017, 79, pp.34-51. ⟨10.1016/j.ultras.2017.02.020⟩
Ultrasonics, 2017, 79, pp.34-51. ⟨10.1016/j.ultras.2017.02.020⟩
ISSN: 0041-624X
Popis: The present research attempts to non-destructively characterize mechanical properties, which are representative of the interfacial adhesion and bond line cohesion of adhesively bonded assemblies, using an ultrasonic method. Eight bonded samples made of two aluminium substrates and of an epoxy-based adhesive layer were manufactured: four in which the adhesive is fully cured (100%) and four in which crosslinking is partial (80%). For each level of curing, four different surface treatments were applied to the aluminium substrates before assembling, in order to vary the quality of adhesion. Ultrasonic plane wave transmission coefficients (UPWTC) were either measured in a water tank, or simulated using the well-known stiffness matrix method that micmics the experiments, to produce input data for the inverse problem. This latest consists in the evaluation of the elastic properties of either the adhesive bond or the interphases between both substrates and the adhesive layer. If the interphases are of nominal quality, the values of the inferred properties of the adhesive bond match those previously measured on individual epoxy samples, whether the epoxy is fully or partially cured. However, when interphases are not of nominal quality level, the optimized bond moduli reveal an apparent anisotropy, although the epoxy layer is known to be isotropic. This apparent anisotropy is explained by an analytical rule of mixture, thus giving confidence in the proposed ultrasonic technique, which is then suggested as a potential way to detect weaknesses of interphases. Finally, the optimization of the interphases elastic properties is carried out. The measured normal and shear stiffnesses are shown to decrease as the interphases get degraded. All ultrasonically-measured parameters (apparent anisotropy of the bond and interfacial stiffnesses) vary monotonically with the bonds strength, which was measured via mechanical tests. The proposed UPWTC method was shown to have a strong potential to distinguish between adhesive and cohesive weaknesses of bonded joints, and to estimate corresponding mechanical properties.
Databáze: OpenAIRE
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