Development and Properties of New Mullite Based Refractory Grog

Autor: Pavel Kovář, Petr Štursa, Lukáš Tvrdík, Karel Lang, Lenka Nevřivová, David Zemánek, Dalibor Všianský, Karel Dvořák, Lucie Keršnerová
Jazyk: angličtina
Rok vydání: 2021
Předmět:
Zdroj: Materials
Volume 14
Issue 4
Materials, Vol 14, Iss 779, p 779 (2021)
Materials . 2021, vol. 14, issue 4, p. 1-15.
ISSN: 1996-1944
DOI: 10.3390/ma14040779
Popis: The presented study is focused on optimization and characterization of a high-alumina refractory aggregate based on natural raw materials—kaolins, claystone, and mullite dust by-product (used to increase the alumina and mullite contents, respectively). In total, four individual formulas with the Al2O3 contents between 45 and 50 wt.% were designed
the samples were subsequently fired, both in a laboratory oven and an industrial tunnel furnace. The effects of repeated firing were examined during industrial pilot tests. Mineral and chemical compositions and microstructures, of both the raw materials and designed aggregates, were thoroughly investigated by the means of X-ray fluorescence spectroscopy, powder X-ray diffraction, and optical and scanning electron microscopies. Porosity, mineral composition, and mullite crystal-size development during the firing process were also studied. Based on the acquired results, the formula with the perspective to be used as a new mullite grog, featuring similar properties as the available commercial products, however, with reduced production expenses, was selected. The quality of grog determines to a large extent the properties of the final product. Hence, optimization of aggregates for specific refractories is of a great importance. The production of engineered aggregates provides the opportunity to utilize industrial by-products.
Databáze: OpenAIRE
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