In situ X-ray crystallographic study of the structural evolution of colloidal crystals upon heating
| Autor: | Zozulya, A.V., Meijer, J.M., Shabalin, A., Ricci, A., Westermeier, F., Kurta, R.P., Lorenz, U., Singer, A., Yefanow, O., Petukhov, A.V., Sprung, M., Vartanyants, I. A., Physical and Colloid Chemistry, Sub Physical and Colloid Chemistry |
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| Přispěvatelé: | Physical and Colloid Chemistry, Sub Physical and Colloid Chemistry |
| Jazyk: | angličtina |
| Rok vydání: | 2013 |
| Předmět: |
Small-angle X-ray scattering
Chemistry Astrophysics::High Energy Astrophysical Phenomena Hard spheres Atmospheric temperature range Colloidal crystal General Biochemistry Genetics and Molecular Biology Synchrotron law.invention Condensed Matter::Soft Condensed Matter Crystallography chemistry.chemical_compound Beamline law Condensed Matter::Superconductivity small-angle X-ray scattering ddc:540 colloidal crystals Polystyrene X-Ray Diffraction and Imaging Glass transition thermal treatment |
| Zdroj: | Journal of applied crystallography 46(4), 903-907 (2013). doi:10.1107/S0021889813003725 Journal of Applied Crystallography, 46, 903. International Union of Crystallography Journal of Applied Crystallography |
| ISSN: | 0021-8898 |
| DOI: | 10.3204/desy-2013-00133 |
| Popis: | Journal of applied crystallography 46(4), 903-907 (2013). doi:10.1107/S0021889813003725 Structural evolution of colloidal crystals made of polystyrene hard spheres hasbeen studied in situ upon incremental heating of a crystal in a temperature rangebelow and above the glass transition temperature of polystyrene. Thin films ofcolloidal crystals having different particle sizes were studied in transmissiongeometry using a high-resolution small-angle X-ray scattering setup at the P10Coherence Beamline of the PETRA III synchrotron facility. The transformationof colloidal crystals to a melted state has been observed in a narrow temperatureinterval of less than 10 K. Published by Munksgaard, Copenhagen |
| Databáze: | OpenAIRE |
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