Hard X-ray Nanotomography of Catalytic Solids at Work
Autor: | Gonzalez-Jimenez, Ines D., Cats, Korneel, Davidian, Thomas, Ruitenbeek, Matthijs, Meirer, Florian, Liu, Yijin, Nelson, Johanna, Andrews, Joy C., Pianetta, Piero, de Groot, Frank M. F., Weckhuysen, Bert M., Sub Inorganic Chemistry and Catalysis, Inorganic Chemistry and Catalysis |
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Přispěvatelé: | Sub Inorganic Chemistry and Catalysis, Inorganic Chemistry and Catalysis |
Rok vydání: | 2012 |
Předmět: |
Fischer-Tropsch catalysis
DECOMPOSITION FISCHER-TROPSCH SYNTHESIS Analytical chemistry Heterogeneous catalysis in situ spectroscopy Catalysis NANOSCALE SYSTEMS Taverne LOWER OLEFINS Chemical composition Nanoscopic scale X-ray absorption spectroscopy Chemistry Resolution (electron density) MICROSCOPY Fischer–Tropsch process General Medicine General Chemistry IRON CATALYSTS heterogeneous catalysis SPECTROMICROSCOPY Particle transmission X-ray microscopy BEHAVIOR |
Zdroj: | Angewandte Chemie-International Edition, 51(48), 11986. John Wiley and Sons Ltd |
ISSN: | 1433-7851 |
DOI: | 10.1002/anie.201204930 |
Popis: | A closer look at catalysis: In situ hard X‐ray nanotomography has been developed (see picture) as a method to investigate an individual iron‐based Fischer–Tropsch‐to‐Olefins (FTO) catalyst particle at elevated temperatures and pressures. 3D and 2D maps of 30 nm resolution could be obtained and show heterogeneities in the pore structure and chemical composition of the catalyst particle of about 20 μm. |
Databáze: | OpenAIRE |
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