Long-chain phenols
| Autor: | John H. P. Tyman, B.A. Colenutt, V. Tychopoulos |
|---|---|
| Rok vydání: | 1984 |
| Předmět: |
Chromatography
biology Anacardium Organic Chemistry General Medicine Reversed-phase chromatography biology.organism_classification Biochemistry High-performance liquid chromatography Analytical Chemistry Solvent chemistry.chemical_compound Adsorption chemistry Gradient elution Phenols Cashew nut Acetonitrile Long chain Quantitative analysis (chemistry) Tetrahydrofuran |
| Zdroj: | Journal of Chromatography A. 303:137-150 |
| ISSN: | 0021-9673 |
| DOI: | 10.1016/s0021-9673(01)96053-4 |
| Popis: | The novel separation of the constituent phenols in technical cashew nut-shell liquid from the industrial processing of Anacardium occidentale has been effected by high-performance liquid chromatography. The adsorption mode on columns of 5-μm and 10-μm Partisil and the reversed-phase partition mode with 5-μm and 10-μm Spherisorb bonded with octadecylsilane have been investigated. Determination of relative molar response values for the main constituent phenols and the use of an internal standard have led to a quantitative procedure by isocratic elution under reversed-phase partition, preferably with the solvent acetonitrile-water. Gradient elution with tetrahydrofuran and acetonitrile has also enabled the polymeric material to be estimated in the various types of technical cashew nut-shell liquid examined. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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