Effects of long-term water storage on the microtensile bond strength of five experimental self-etching adhesives based on surfactants rather than HEMA
Autor: | Carlo Prati, Cesar Henrique Zanchi, Eliseu Aldrighi Münchow, Evandro Piva, Fabrício Aulo Ogliari, Stefano Chersoni, Rodrigo Varella de Carvalho, Flávio Fernando Demarco |
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Přispěvatelé: | Zanchi CH, Münchow EA, Ogliari FA, de Carvalho RV, Chersoni S, Prati C, Demarco FF, Piva E |
Rok vydání: | 2012 |
Předmět: |
Dental Stress Analysis
adhesive Drug Storage Dentistry Methacrylate Statistics Nonparametric Polyethylene Glycols Surface-Active Agents chemistry.chemical_compound Pulmonary surfactant Tensile Strength PEG ratio Dentin medicine Animals Composite material General Dentistry PEG 400 Analysis of Variance Bond strength business.industry Dental Bonding Water monomer UDMA Resin Cements Cross-Linking Reagents medicine.anatomical_structure chemistry Dentin-Bonding Agents Methacrylates Cattle Adhesive business |
Zdroj: | Clinical Oral Investigations. 17:833-839 |
ISSN: | 1436-3771 1432-6981 |
DOI: | 10.1007/s00784-012-0791-4 |
Popis: | OBJECTIVES: The purpose of this study is to evaluate the hypothesis that replacing 2-hydroxyethyl methacrylate (HEMA) for surfactant dimethacrylates (SD) does not affect the immediate and long-term microtensile bond strength (μTBS) of experimental two-step self-etch HEMA-free adhesive systems applied on dentin. MATERIALS AND METHODS: Five experimental HEMA-free two-step self-etching systems containing different SD (ethoxylated bisphenol A diglycidyl dimethacrylate (Bis-EMA 10, B10), Bis-EMA 30 (B30), poly-ethyleneglycol (400) dimethacrylate (PEG 400, P400), PEG 1000 (P1000), and PEG 400 urethane dimethacrylate (UDMA) (UP400)) and a HEMA-containing system (control) (HA) were formulated. Specimens were subjected to the μTBS test after 24 h and 6 and 12 months of storage. Data (in megapascals) were analyzed by Kruskal-Wallis and Dunn tests (α = 0.05). RESULTS: Medians of the μTBS data after 24 h of storage are: HA = 57.2(A), B10 = 26.2(BC), B30 = 24.0(C), P400 = 32.6(BC), P1000 = 37.3(B), and UP400 = 57.9(A); after 6 months are: HA = 47.9(A), B10 = 18.5(B), B30 = 7.8(C), P400 = 16.1(B), P1000 = 14.6(BC), and UP400 = 51.6(A); and after 12 months are: HA = 31.2(A), B10 = 15.2(B), B30 = 9.0(B), P400 = 9.1(B), P1000 = 13.3(B), and UP400 = 35.7(A). Between the HEMA-free groups, the adhesive system formulated with PEG 400 UDMA produced similar μTBS to the HEMA-containing group. Also, the storage of specimens decreased the μTBS (p |
Databáze: | OpenAIRE |
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