Copper Oxide Nanoparticles Synthesis by Electrochemical Method
| Autor: | Nitin R. Dighore, Anjali S. Rajbhoj, Suresh T. Gaikwad, Sunita Jadhav |
|---|---|
| Jazyk: | angličtina |
| Rok vydání: | 2016 |
| Předmět: |
0106 biological sciences
lcsh:TN1-997 Ammonium bromide current density Materials science Electrolytic cell Inorganic chemistry chemistry.chemical_element Nanoparticle Electrochemistry 01 natural sciences 010309 optics copper oxide nanoparticles chemistry.chemical_compound tetra alkyl ammonium bromide 010608 biotechnology 0103 physical sciences General Materials Science Acetonitrile lcsh:Mining engineering. Metallurgy biology electrochemical method current density tetra alkyl ammonium bromide copper oxide nanoparticles biology.organism_classification Anode chemistry Tetra Platinum electrochemical method |
| Zdroj: | Medžiagotyra, Vol 22, Iss 2, Pp 170-173 (2016) |
| ISSN: | 2029-7289 1392-1320 |
| Popis: | Copper oxide nanoparticles were prepared by electrochemical reduction method which is environmental benign. Tetra ethyl ammonium bromide (TEAB), tetra propyl ammonium bromide (TPAB), tetra butyl ammonium bromide (TBAB) were used as stabilizing agent in an organic medium viz. tetra hydro furan (THF) and acetonitrile (ACN) in 4:1 ratio by optimizing current density. The reduction process takes place under atmospheric condition over a period of 2 h. Such nanoparticles were prepared using simple electrolysis cell in which the sacrificial anode was a commercially available copper metal sheet and platinum (inert) sheet acted as a cathode. The stabilizers were used to control the size of a nanoparticles. The synthesized copper oxide nanoparticles were characterized by using UV-Visible, FT-IR, XRD, SEM-EDS and TEM analysis techniques.DOI: http://dx.doi.org/10.5755/j01.ms.22.2.7501 |
| Databáze: | OpenAIRE |
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