Optimization of Glutathione Adhesion Process to Modified Graphene Surfaces
| Autor: | Dorota Nowak, M. Czerniak-Reczulska, Witold Jakubowski, Marian Clapa, Anna Sobczyk-Guzenda, Radomir Atraszkiewicz, Damian Batory, Tomasz Warga, Witold Szymanski, Piotr Kula, Łukasz Kaczmarek |
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| Jazyk: | angličtina |
| Rok vydání: | 2021 |
| Předmět: |
biomedical applications
Materials science Graphene Scanning electron microscope General Chemical Engineering Chemical structure graphene biofunctionalization Infrared spectroscopy Article law.invention lcsh:Chemistry symbols.namesake n/a Chemical engineering lcsh:QD1-999 law symbols Surface modification Peptide bond General Materials Science glutathione Fourier transform infrared spectroscopy Raman spectroscopy |
| Zdroj: | Nanomaterials Volume 11 Issue 3 Nanomaterials, Vol 11, Iss 756, p 756 (2021) |
| ISSN: | 2079-4991 |
| DOI: | 10.3390/nano11030756 |
| Popis: | The presented work shows the results of the functionalization of the graphene surface obtained by the growth on the liquid bimetallic matrices method. We used glutathione (GSH) as a peptide model, which allowed us to optimize the procedure to obtain high process efficiency. To establish the amount of GSH attached to the graphene surface, the Folina-Ciocalteu method was used, which allows the assessment of the concentration of colored reaction products with peptide bonds without the disadvantages of most methods based on direct colored reaction of peptide bonds. Samples surface morphology, quality of graphene and chemical structure in the subsequent stages of surface modification were tested—for this purpose Raman spectroscopy, scanning electron microscopy (SEM), and Fourier-transform infrared spectroscopy (FTIR) were used. |
| Databáze: | OpenAIRE |
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