Validation interlaboratory trial for ISO 12010 : water quality-determination of short-chain polychlorinated alkanes (SCCP) in water
| Autor: | Josep Caixach, Moana Engelke, Theodor Prey, Dirk Loeffler, Sabine Geiss, Ines Hussy, Alexander Ruderisch, Jorge E. Olmos, Philipp Steinbichl, Gerhild Donnevert, Tom Schillings, Aurélien Rey, Birgit Koerner, Sigrid Scharf, Juergen W. Einax, Bettina Hilger, Herbert Lepper, Nicole Lettmann, F. Javier Santos, George Sawal, Max Schneider, Marie-Pierre Strub, Arantxa Bartolomé, Hervé Adrien |
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| Přispěvatelé: | Thuringer Landesanstalt fur Umwelt und Geologie, Thüringer Landesanstalt für Umwelt und Geologie, Lehrbereich Umweltanalytik, Friedrich-Schiller-Universität = Friedrich Schiller University Jena [Jena, Germany], Technische Hochschule Mittelhessen - University of Applied Sciences [Giessen] (THM), Ruhrverband, CTC, Landesanstalt fur Umwelt Messungen und Naturschutz Baden-Wurttemberg, Abteilung Analytik, Technologiezentrum Wasser, FTU Forschungsgesellschaft Technischer, Umweltschutz GmbH, Bayerisches Landesamt fur Gesundheit und Lebensmittelsicherheit, Sachgebiet Chemikaliensicherheit und Toxikologie, Landeslabor Berlin-Brandenburg, Institut National de l'Environnement Industriel et des Risques (INERIS), Übergreifende Angelegenheiten der Luftreinhaltung, Umweltbundesamt, Bundesanstalt fur Gewasserkunde, Bundesanstalt für Gewässerkunde, Landesbetrieb fur Hochwasserschutz und Wasserwirtschaft, Marine Laboratory, Scottish Government, Agrolab Labor GmbH, Department of Analytical Chemistry, University of Barcelona, Institute of Environmental Assessment and Water Research (IDAEA), Consejo Superior de Investigaciones Científicas [Madrid] (CSIC) |
| Jazyk: | angličtina |
| Rok vydání: | 2012 |
| Předmět: |
ISO 12010
General Chemical Engineering Analytical chemistry 010501 environmental sciences Mass spectrometry 01 natural sciences CHLOROPARAFFINS EUROPEAN WATER FRAMEWORK DIRECTIVE Safety Risk Reliability and Quality Instrumentation 0105 earth and related environmental sciences Reproducibility PCA Chromatography PRIORITY SUBSTANCES Chemistry 010401 analytical chemistry Extraction (chemistry) General Chemistry 6. Clean water 0104 chemical sciences Clean-up Wastewater 13. Climate action CHLOROALKANES C-10-C-13 [SDE]Environmental Sciences Gas chromatography Water quality Surface water SCCP |
| Zdroj: | Accreditation and Quality Assurance Accreditation and Quality Assurance, Springer Verlag, 2012, 17 (1), pp.15-25. ⟨10.1007/s00769-011-0820-z⟩ |
| ISSN: | 0949-1775 1432-0517 |
| Popis: | International audience; A validation interlaboratory trial was carried out to prepare ISO 12010: Water quality-Determination of short-chain polychlorinated alkanes (SCCP) in water-Method using gas chromatography/mass spectrometry (GC-MS) and electron capture negative ionisation (ECNI). The task was to determine the sum of short-chain polychlorinated n-alkanes with carbon chain lengths of C-10-C-13 and a chlorine content between 49% (g/100 g) and 67% (g/100 g) in water by GC-ECNI-MS. The quantification had to be performed by multiple linear regression as described in ISO/DIS 12010, the compulsory method. Samples distributed were real river samples, and waste water spiked with a target concentration of 0.4 and 0.6 mu g/L for the sum of SCCPs, i.e. a concentration around the environmental quality target level according to the European Water Framework Directive. The different types of water samples tested were surface water with |
| Databáze: | OpenAIRE |
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