Determination of Glycarbylamide Residues in Chicken Tissues by HPLC with Post-Column Reaction

Autor: Noriko Tazima, Takashi Horiuchi, Tatsuro Sekiya, Yasuharu Mizuno, Masako Maeda, Kouko Hamamoto
Rok vydání: 2006
Předmět:
Zdroj: Journal of the Food Hygienic Society of Japan (Shokuhin Eiseigaku Zasshi). 47:293-296
ISSN: 1882-1006
0015-6426
DOI: 10.3358/shokueishi.47.293
Popis: A newly developed HPLC method for determination of glycarbylamide (GB) in chicken liver was applied to other tissues (muscle, fat and kidney). The recoveries of GB in muscle, fat and kidney were 87.2% (CV 0.5), 91.3% (CV 4.7), 79.7% (CV 1.0), respectively. The detection limit of GB was 0.01 ppm. GB concentrations were determined by this method in tissues (muscle, fat, liver and kidney) from chickens sacrificed 5 days after oral administration of GB mixed in feed at 60 mg/kg of feed for 7 days. GB was not detected in these chicken tissues.
Databáze: OpenAIRE