Simultaneous Determination of 10 Ultratrace Elements in Infant Formula, Adult Nutritionals, and Milk Products by ICP/MS After Pressure Digestion: Single-Laboratory Validation
| Autor: | Stéphane Dubascoux, Eric Poitevin, Janique Richoz Payot, Marine Nicolas, Celine Fragniere Rime |
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| Rok vydání: | 2015 |
| Předmět: |
Adult
inorganic chemicals chemistry.chemical_element Mass Spectrometry Analytical Chemistry Pressure Humans Environmental Chemistry Sample preparation Microwave digestion Inductively coupled plasma mass spectrometry Arsenic Pharmacology Chromatography Spectrophotometry Atomic Infant Formula Trace Elements Mercury (element) chemistry Ashing Dairy Products Inductively coupled plasma Laboratories Agronomy and Crop Science Selenium Food Science |
| Zdroj: | Journal of AOAC INTERNATIONAL. 98:953-961 |
| ISSN: | 1944-7922 1060-3271 |
| Popis: | A single-laboratory validation (SLV) is presented for the simultaneous determination of 10 ultratrace elements (UTEs) including aluminum (Al), arsenic (As), cadmium (Cd), cobalt (Co), chromium (Cr), mercury (Hg), molybdenum (Mo), lead (Pb), selenium (Se), and tin (Sn) in infant formulas, adult nutritionals, and milk based products by inductively coupled plasma (ICP)/MS after acidic pressure digestion. This robust and routine multielemental method is based on several official methods with modifications of sample preparation using either microwave digestion or high pressure ashing and of analytical conditions using ICP/MS with collision cell technology. This SLV fulfills AOAC method performance criteria in terms of linearity, specificity, sensitivity, precision, and accuracy and fully answers most international regulation limits for trace contaminants and/or recommended nutrient levels established for 10 UTEs in targeted matrixes. |
| Databáze: | OpenAIRE |
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