Endocrine disrupting chemicals in fish bile: A rapid method of analysis using English sole (Parophrys vetulus) from Puget Sound, WA, USA
| Autor: | Sandra M. O'Neill, Gina M. Ylitalo, Jon Buzitis, James E. West, Tracy K. Collier, Denis A.M. da Silva, Lyndal L. Johnson, William L. Reichert |
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| Rok vydání: | 2013 |
| Předmět: |
Male
Washington Time Factors Environmental Engineering Oceans and Seas Health Toxicology and Mutagenesis Endocrine Disruptors Limit of Detection Lc ms ms Animals Bile Environmental Chemistry 17α-ethynylestradiol Cities Sound (geography) geography geography.geographical_feature_category biology Chemistry Hydrolysis Public Health Environmental and Occupational Health Reproducibility of Results English sole General Medicine General Chemistry Method of analysis biology.organism_classification Pollution Environmental chemistry Flatfishes Fish Environmental Monitoring |
| Zdroj: | Chemosphere. 92:1550-1556 |
| ISSN: | 0045-6535 |
| Popis: | This study describes a recently developed and rapid method to measure bisphenol A (BPA), 17β-estradiol (E2) and 17α-ethynylestradiol (EE2) in bile of fish using enzymatic hydrolysis of samples followed by solid-phase extraction and ultra-performance liquid chromatography with tandem mass spectrometry. The limits of quantitation (LOQ) for BPA, EE2 and E2 were 6.3 ng mL−1, 12.5 ng mL−1 and 6.3 ng mL−1, respectively. These compounds were analyzed in bile of male English sole (Parophrys vetulus) collected from urban and non-urban sites in Puget Sound, WA, USA. The BPA and E2 concentrations (and occurrence) ranged from |
| Databáze: | OpenAIRE |
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