Continuous or Batch Solid-Liquid Extraction of Antioxidant Compounds from Seeds of Sterculia apetala Plant and Kinetic Release Study
Autor: | Juliana Villasante, Gádor Indra Hidalgo, María Pilar Almajano, Federica Mosca |
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Přispěvatelé: | Universitat Politècnica de Catalunya. Departament d'Enginyeria Química |
Jazyk: | angličtina |
Rok vydání: | 2018 |
Předmět: |
0106 biological sciences
Diffusion Sterculia Pharmaceutical Science Sterculia apetala continuous extraction 01 natural sciences fatty acids Article Antioxidants Analytical Chemistry lcsh:QD241-441 chemistry.chemical_compound Enginyeria química [Àrees temàtiques de la UPC] lcsh:Organic chemistry 010608 biotechnology Drug Discovery Solid phase extraction Physical and Theoretical Chemistry Chromatography ABTS Ethanol biology Chemistry 010401 analytical chemistry Organic Chemistry Extraction (chemistry) Water biology.organism_classification 0104 chemical sciences Solvent Chemistry (miscellaneous) Seeds Molecular Medicine kinetic diffusion Gas chromatography natural antioxidant |
Zdroj: | Molecules Volume 23 Issue 7 Molecules, Vol 23, Iss 7, p 1759 (2018) UPCommons. Portal del coneixement obert de la UPC Universitat Politècnica de Catalunya (UPC) Molecules : A Journal of Synthetic Chemistry and Natural Product Chemistry Recercat. Dipósit de la Recerca de Catalunya instname |
ISSN: | 1420-3049 |
DOI: | 10.3390/molecules23071759 |
Popis: | This work has been intended to investigate the antioxidant properties of compounds extracted from seeds of Sterculia apetala (a plant from Central America) in order to add further results to the relatively poor existing literature on the beneficial properties of this plant. Different extraction methodologies were used such as batch or continuous extraction conditions using water or ethanol 50% as solvents. The kinetic study has allowed estimation of the effective diffusion coefficients in a continuous solid-liquid extraction, highlighting the strict dependence of the diffusion rate and temperature and kind of solvent, showing the highest diffusion rate with ethanol 50% at 60 ° C. The comparison between different techniques and two solvents led to the selection of water as the best extraction solvent while batch mechanically-agitated extraction was the most efficient mode, with the benefits of use of an environmental-friendly solvent and reduction in process time to achieve a high amount of extracted phenolic compounds. The analysis techniques used were ABTS and Folin-Ciocalteau methods to investigate the antioxidant activity and quantify the Total Phenolic Content (TPC) respectively. Also, different fatty acids were extracted from Sterculia apetala seeds and analysed by Gas Chromatography in order to quantify other interesting chemical species besides antioxidants. |
Databáze: | OpenAIRE |
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