Multiresidue analysis of pesticides, polyaromatic hydrocarbons and polychlorinated biphenyls in poultry meat and chicken eggs by GC-MS/MS: method development and validation

Autor:	Reshma Patil, Niladri Sekhar Chatterjee, Narayan Kamble, Apurva Nerpagar, Nagnath Langade, Chandrasekar Kandaswamy, S. I. Davis Presley, Kaushik Banerjee
Rok vydání:	2022
Předmět:	Meat Solid Phase Extraction Pesticide Residues Reproducibility of Results General Medicine Pollution Polychlorinated Biphenyls Gas Chromatography-Mass Spectrometry Poultry Tandem Mass Spectrometry Animals Pesticides Chickens Food Science
Zdroj:	Journal of environmental science and health. Part. B, Pesticides, food contaminants, and agricultural wastes. 57(4)
ISSN:	1532-4109
Popis:	The study uses gas chromatography with tandem mass spectrometry (GC-MS/MS) to develop a reliable analytical approach for detecting multiclass pesticides, polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs) in poultry meat and chicken eggs. The meat (2 g) and egg (4 g) samples were extracted with acidified acetonitrile (10 mL) as part of the optimized sample preparation technique. The cleanup consisted of freezing an aliquot of the extract (5 mL) at -20 °C, followed by dispersive solid phase extraction using 50 mg PSA + 100 mg C
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::30cc0c23a0fe9bc0af31f1c33826c74e https://pubmed.ncbi.nlm.nih.gov/35452352 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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