Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12)
| Autor: | Evamarie Hey-Hawkins, Peter Lönnecke, Max Milewski, Anne-marie Caminade |
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| Přispěvatelé: | Leipzig University, Laboratoire de chimie de coordination (LCC), Institut de Chimie de Toulouse (ICT), Institut de Recherche pour le Développement (IRD)-Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Université de Toulouse (UT)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS)-Institut National Polytechnique (Toulouse) (Toulouse INP), Université de Toulouse (UT)-Institut de Recherche pour le Développement (IRD)-Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Centre National de la Recherche Scientifique (CNRS), German Research Foundation, European Project: 860322,H2020-EU.1.3.1.,H2020-MSCA-ITN-2019,CCIMC(2020) |
| Jazyk: | angličtina |
| Rok vydání: | 2022 |
| Předmět: | |
| Zdroj: | Acta crystallographica Section E : Crystallographic communications [2015-...] Acta crystallographica Section E : Crystallographic communications [2015-..], 2022, 78 (12), pp.1145-1150. ⟨10.1107/S205698902201043X⟩ |
| ISSN: | 2056-9890 |
| DOI: | 10.1107/S205698902201043X⟩ |
| Popis: | Automated X-ray data recording and data reduction strategies are straightforward and powerful these days, as well as semi-automated routines to solve standard structures without, or at least with only little manual intervention and within a relatively short time. The structure determination of the amino-carborane closo-9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12), C22H29B10N, is an example that automated routines still always have to be revised and that it may be necessary to be aware of possible problems of a structure determination. |
| Databáze: | OpenAIRE |
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