An Innovative Synthesis of Nano-ZSM-5 Zeolite Through Interrupted Ultrasound

Autor:	Pirzada Afridi, Siddiqui, Farrukh Arsalan, Gonzalez-Cortes, Sergio, France, Liam
Rok vydání:	2021
Předmět:	Chemistry Applied Zeolite Zeolite Hydrothermal Treatment Nano-ZSM-5 Interrupted Ultrasound Physisorption Interrupted Ultrasound Nano-ZSM-5 Physisorption Kimya Uygulamalı Hydrothermal Treatment
Zdroj:	Volume: 6, Issue: 1 15-23 Journal of Ongoing Chemical Research
ISSN:	2651-4338
DOI:	10.5281/zenodo.5564497
Popis:	NanoZSM-5 was synthesized with crystal size ≤30 nm by using an interrupted ultrasound crystallization process. In his process, the hydrothermal treatment was interrupted with ultrasound and without ultrasound at 170oC for 24 hours. The nanoZSM-5 crystallinity was confirmed by X-ray diffraction. The crystallite size and morphology were determined by TEM and SEM. The textural properties were investigated by N2physisorption.29Si MAS NMR confirmed the framework composition and presence of silanol group at the surface of the nanoZSM-5.
Databáze:	OpenAIRE
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