Exploiting In Situ Solid-State NMR for the Discovery of New Polymorphs during Crystallization Processes

Autor:	Colan E. Hughes, Philip Andrew Williams, Thomas Roper Peskett, Kenneth D. M. Harris
Rok vydání:	2012
Předmět:	In situ Materials science Oxide Nanotechnology law.invention chemistry.chemical_compound Molecular solid Solid-state nuclear magnetic resonance chemistry Chemical engineering Polymorphism (materials science) law General Materials Science Physical and Theoretical Chemistry Crystallization
Zdroj:	The Journal of Physical Chemistry Letters. 3:3176-3181
ISSN:	1948-7185
DOI:	10.1021/jz301252u
Popis:	We report the discovery of new polymorphic forms of solids by exploiting a solid-state NMR technique that has been developed for in situ monitoring of the evolution of crystallization processes. The capability of the technique to reveal the existence of new polymorphic forms of molecular solids is illustrated by the discovery of two new polymorphs of methyldiphenylphosphine oxide and a new solid form of the 1,10-dihydroxydecane/urea system.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::2cfbe0ebe96673ad4a29235de54835f1 https://doi.org/10.1021/jz301252u Zobrazit plný text záznamu