Antifungal residues analysis in various Romanian honey samples analysis by high resolution mass spectrometry
Autor: | Caterina Dumitru, Elena Lacramioara Lisa, Daniela Borda, Carmen Lidia Chițescu, Giorgiana-Valentina Blaga, Camelia Vizireanu |
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Rok vydání: | 2020 |
Předmět: |
Antifungal
medicine.drug_class Food Contamination Environmental pollution 010501 environmental sciences 01 natural sciences Tandem Mass Spectrometry medicine Pesticides Routine analysis 0105 earth and related environmental sciences Romania 010401 analytical chemistry food and beverages Honey General Medicine Contamination Pesticide Pollution Honey samples Fungicides Industrial 0104 chemical sciences Environmental chemistry Environmental science Food Analysis Chromatography Liquid Food Science Food contaminant |
Zdroj: | Journal of Environmental Science and Health, Part B. 55:484-494 |
ISSN: | 1532-4109 0360-1234 |
DOI: | 10.1080/03601234.2020.1724016 |
Popis: | Given that the pesticide and fungicide residues determination in honey is not a routine analysis in Romania, information on these emerging contaminants is useful for consumer's safety. High resolution mass spectrometry technique was applied by Q-Exactive Orbitrap LC-MS/MS to identify and quantify environmental contaminants in honey. A list of 25 compounds, biocides and antifungals was selected for the method development, based on the occurrence in the Romanian environment and their potential usage in agriculture. The method was applied for 18 various honey samples collected in different geographic regions of Romania. Eleven compounds were present in the honey samples: carbendazim, enilconazole, hexaconazole, penconazole, tebuconazole, flusilazole, thiabendazole, terconazole, cyproconazole, propiconazole, metalaxyl. Targeted MS/MS analyses were performed for confirmation. The measured quantities ranged from 1.7-7.2 μg kg |
Databáze: | OpenAIRE |
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