Antifungal residues analysis in various Romanian honey samples analysis by high resolution mass spectrometry

Autor: Caterina Dumitru, Elena Lacramioara Lisa, Daniela Borda, Carmen Lidia Chițescu, Giorgiana-Valentina Blaga, Camelia Vizireanu
Rok vydání: 2020
Předmět:
Zdroj: Journal of Environmental Science and Health, Part B. 55:484-494
ISSN: 1532-4109
0360-1234
DOI: 10.1080/03601234.2020.1724016
Popis: Given that the pesticide and fungicide residues determination in honey is not a routine analysis in Romania, information on these emerging contaminants is useful for consumer's safety. High resolution mass spectrometry technique was applied by Q-Exactive Orbitrap LC-MS/MS to identify and quantify environmental contaminants in honey. A list of 25 compounds, biocides and antifungals was selected for the method development, based on the occurrence in the Romanian environment and their potential usage in agriculture. The method was applied for 18 various honey samples collected in different geographic regions of Romania. Eleven compounds were present in the honey samples: carbendazim, enilconazole, hexaconazole, penconazole, tebuconazole, flusilazole, thiabendazole, terconazole, cyproconazole, propiconazole, metalaxyl. Targeted MS/MS analyses were performed for confirmation. The measured quantities ranged from 1.7-7.2 μg kg
Databáze: OpenAIRE
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