A 31T split-pair pulsed magnet for single crystal x-ray diffraction at low temperature
| Autor: | Fabienne Duc, J. Béard, Lin Zhang, Carsten Detlefs, Thomas Roth, G. L. J. A. Rikken, Marc Nardone, A. Zitouni, X. Fabrèges, J.-P. Nicolin, M. Lesourd, P. Delescluse, J. Billette, P. Frings |
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| Přispěvatelé: | Laboratoire national des champs magnétiques intenses - Toulouse (LNCMI-T), Institut National des Sciences Appliquées - Toulouse (INSA Toulouse), Institut National des Sciences Appliquées (INSA)-Université de Toulouse (UT)-Institut National des Sciences Appliquées (INSA)-Université de Toulouse (UT)-Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Centre National de la Recherche Scientifique (CNRS)-Université Grenoble Alpes [2016-2019] (UGA [2016-2019]), Laboratoire Léon Brillouin (LLB - UMR 12), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay-Centre National de la Recherche Scientifique (CNRS), European Synchrotron Radiation Facility (ESRF), European XFEL GmbH (XFEL), European XFEL GmbH, Université Toulouse III - Paul Sabatier (UT3), Université Fédérale Toulouse Midi-Pyrénées-Université Fédérale Toulouse Midi-Pyrénées-Centre National de la Recherche Scientifique (CNRS)-Université Grenoble Alpes [2016-2019] (UGA [2016-2019])-Institut National des Sciences Appliquées - Toulouse (INSA Toulouse), Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Centre National de la Recherche Scientifique (CNRS)-Université Paris-Saclay |
| Jazyk: | angličtina |
| Rok vydání: | 2014 |
| Předmět: |
Cryostat
Diffraction Physics - Instrumentation and Detectors Materials science FOS: Physical sciences 02 engineering and technology 7. Clean energy 01 natural sciences law.invention Condensed Matter - Strongly Correlated Electrons Optics law 0103 physical sciences ddc:530 [PHYS.PHYS.PHYS-INS-DET]Physics [physics]/Physics [physics]/Instrumentation and Detectors [physics.ins-det] 010306 general physics Instrumentation Strongly Correlated Electrons (cond-mat.str-el) business.industry Particle accelerator Instrumentation and Detectors (physics.ins-det) 021001 nanoscience & nanotechnology Synchrotron Beamline Magnet X-ray crystallography Xray single crystal diffraction- High pulsed field- split pair magnet-Low temperature [PHYS.COND.CM-SCE]Physics [physics]/Condensed Matter [cond-mat]/Strongly Correlated Electrons [cond-mat.str-el] 0210 nano-technology business Single crystal |
| Zdroj: | Review of scientific instruments 85(5), 053905 (2014). doi:10.1063/1.4878915 |
| DOI: | 10.1063/1.4878915 |
| Popis: | We have developed a pulsed magnet system with panoramic access for synchrotron x-ray diffraction in magnetic fields up to 31T and at low temperature down to 1.5 K. The apparatus consists of a split-pair magnet, a liquid nitrogen bath to cool the pulsed coil, and a helium cryostat allowing sample temperatures from 1.5 up to 250 K. Using a 1.15MJ mobile generator, magnetic field pulses of 60 ms length were generated in the magnet, with a rise time of 16.5 ms and a repetition rate of 2 pulses/hour at 31 T. The setup was validated for single crystal diffraction on the ESRF beamline ID06. |
| Databáze: | OpenAIRE |
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