Vibrational study and thermal behavior of dihydrogenotriphosphate trihydrate of 4-aminobenzoic acid and its anhydrous new form fertilizer type NP

Autor:	Ismail Fahim, Soufiane Zerraf, Malika Tridane, Mustapha Belhabra, Said Belaaouad, Khadija El Kababi, Azzedine Atibi, A. Ouasri, Mohammed Radid
Rok vydání:	2019
Předmět:	General Chemistry Triclinic crystal system Kinetic energy medicine.disease Mass spectrometry Chemical synthesis lcsh:Chemistry chemistry.chemical_compound lcsh:QD1-999 chemistry 4-Aminobenzoic acid medicine Anhydrous Dehydration Hydrate Nuclear chemistry
Zdroj:	Mediterranean Journal of Chemistry, Vol 8, Iss 4, Pp 270-282 (2019)
ISSN:	2028-3997
Popis:	Chemical synthesis methods and IR spectrometry studies are reported for an organic triphosphate (NH3C6H4COOH)3H2P3O10.3H2O and its anhydrous new form NH3C6H4COOH)3H2P3O10. The hydrate compound (NH3C6H4COOH)3H2P3O10.3H2O was synthetized by the ion-exchange resin method. The dehydration of (NH3C6H4COOH)3H2P3O10.3H2O leads at 130°C to (NH3C6H4COOH)3H2P3O10 crystallizing in the triclinic system with space group P 1 (Z = 2) [a = 14.566(6) Å, b = 6.866 (1) Å, c = 6.445 (6) Å, α = 112.36 (3) °, β = 94.51 (1) °, γ = 95.94(7) °, and V = 587.98 (1) Å3]. Merit’s figures are M (10) = 91.9 and F (10) = 55.6 (0.0032, 56). Its thermal behavior and kinetic study were studied by using thermal analyses TGA and DTA techniques between 25 and 600°C.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::2609c1c9069a6cdd8c3288964b20c45b https://doi.org/10.13171/mjc841905308mb Zobrazit plný text záznamu