Deep eutectic solvents (DES) mediated extraction of pectin from Averrhoa bilimbi: Optimization and characterization studies
| Autor: | Rizana Yusof, Muhammad Hakimin Shafie, Chee-Yuen Gan |
|---|---|
| Rok vydání: | 2019 |
| Předmět: |
Averrhoa
Antioxidant food.ingredient Polymers and Plastics Averrhoa bilimbi Pectin medicine.medical_treatment 02 engineering and technology 010402 general chemistry 01 natural sciences chemistry.chemical_compound food Materials Chemistry medicine Eutectic system Chromatography Chemistry Solid Phase Extraction Organic Chemistry Extraction (chemistry) Temperature Free Radical Scavengers Hydrogen-Ion Concentration 021001 nanoscience & nanotechnology 0104 chemical sciences Deep eutectic solvent Solubility Fruit Yield (chemistry) Solvents Pectins Ferric 0210 nano-technology medicine.drug |
| Zdroj: | Carbohydrate Polymers. 216:303-311 |
| ISSN: | 0144-8617 |
| DOI: | 10.1016/j.carbpol.2019.04.007 |
| Popis: | The Box–Behnken design was applied to optimize the extraction of pectin from Averrhoa bilimbi (ABP) using deep eutectic solvents (DES). The four variables of extraction were percentage of DES (X1), extraction time (X2), temperature (X3), and molar ratio of DES components (X4). The quadratic regression equation was established as a predicted model with R2 value of 0.9375. The optimal condition was X1 = 3.74% (w/v), X2 = 2.5 h, X3 = 80 °C, and X4 = 1:1. No significant difference between the predicted (14.70%) and experimental (14.44%) maximum yield of sample was noted. Characterization of physico-chemical properties characterization of ABP was performed. The main components of ABP were galacturonic acids, arabinoses, and xyloses. ABP also showed good functional properties such as water holding capacity (3.70 g/g), oil holding capacity (2.40 g/g), and foaming capacity (133.33%). The results also showed that ABP exhibited free radical scavenging activity (41.46%) and ferric reducing antioxidant power (1.15 mM). |
| Databáze: | OpenAIRE |
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