Pesticide residues determination in Polish organic crops in 2007-2010 applying gas chromatography-tandem quadrupole mass spectrometry
| Autor: | B. Gnusowski, Stanisław Walorczyk, Dorota Remlein-Starosta, Dariusz Drożdżyński, Monika Przewoźniak, A. Ziolkowski, Jolanta Kowalska |
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| Rok vydání: | 2012 |
| Předmět: |
Chromatography
Pesticide residue Tandem Chemistry Analytical technique Pesticide Residues Food Contamination General Medicine Pesticide Tandem mass spectrometry Mass spectrometry Gas Chromatography-Mass Spectrometry Analytical Chemistry Tandem Mass Spectrometry Vegetables Food Organic Gas chromatography Poland Gas chromatography–mass spectrometry Edible Grain Food Science |
| Zdroj: | Food chemistry. 139(1-4) |
| ISSN: | 1873-7072 |
| Popis: | A sensitive, accurate and reliable multiresidue method based on the application of gas chromatography-tandem quadrupole mass spectrometry (GC-QqQ-MS/MS) has been established for screening, identification and quantification of a large number of pesticide residues in produce. The method was accredited in compliance with PN-EN ISO/IEC 17025:2005 standard and it was operated under flexible scope as PB-11 method. The flexible scope of accreditation allowed for minor modifications and extension of the analytical scope while using the same analytical technique. During the years 2007-2010, the method was used for the purpose of verification of organic crop production by multiresidue analysis for the presence of pesticides. A total of 528 samples of differing matrices such as fruits, vegetables, cereals, plant leaves and other green parts were analysed, of which 4.4% samples contained pesticide residues above the threshold value of 0.01 mg/kg. A total of 20 different pesticide residues were determined in the samples. |
| Databáze: | OpenAIRE |
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