Effect of Microwave Heating Conditions on the Preparation of High Surface Area Activated Carbon from Waste Bamboo
| Autor: | Shixing Wang, Xia Yi, Jinhui Peng, Zhaoqiang Zheng, Libo Zhang, Zhang Shengzhou, Hongying Xia, Jian Wu |
|---|---|
| Rok vydání: | 2015 |
| Předmět: |
Technology
Bamboo Materials science Chemical technology Metallurgy microwave heating Chemicals: Manufacture use etc TP200-248 TP1-1185 Condensed Matter Physics waste bamboo Mechanics of Materials Microwave heating medicine 81.05.rm High surface area General Materials Science high surface area activated carbon Physical and Theoretical Chemistry Activated carbon medicine.drug |
| Zdroj: | High Temperature Materials and Processes, Vol 34, Iss 7, Pp 667-674 (2015) |
| ISSN: | 2191-0324 0334-6455 |
| DOI: | 10.1515/htmp-2014-0096 |
| Popis: | The present study reports the effect of microwave power and microwave heating time on activated carbon adsorption ability. The waste bamboo was used to preparing high surface area activated carbon via microwave heating. The bamboo was carbonized for 2 h at 600°C to be used as the raw material. According to the results, microwave power and microwave heating time had a significant impact on the activating effect. The optimal KOH/C ratio of 4 was identified when microwave power and microwave heating time were 700 W and 15 min, respectively. Under the optimal conditions, surface area was estimated to be 3441 m2/g with pore volume of 2.093 ml/g and the significant proportion of activated carbon was microporous (62.3%). The results of Fourier transform infrared spectroscopy (FTIR) were illustrated that activated carbon surface had abundant functional groups. Additionally the pore structure is characterized using Scanning Electron Microscope (SEM). |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|