Structural Analysis of Partially Acetylated Glycosides by Refocused-Decoupled Insensitive Nuclei Enhanced by Polarization Transfer (INEPT) Experiments: A Qualitative and Quantitative Method
Autor: | Max Ratier, Michel Pétraud, Jean-Claude Lartigue, Laurent Pouységu, Bernard De Jeso |
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Rok vydání: | 2002 |
Předmět: |
chemistry.chemical_classification
Molecular Structure Chemistry Stereochemistry Carbohydrate chemistry Carbon-13 Acetylation Pulse sequence Glycosidic bond General Chemistry General Medicine Nuclear magnetic resonance spectroscopy Carbon-13 NMR Computational chemistry Drug Discovery Glycosides Insensitive nuclei enhanced by polarization transfer Spectroscopy Nuclear Magnetic Resonance Biomolecular |
Zdroj: | CHEMICAL & PHARMACEUTICAL BULLETIN. 50:1114-1117 |
ISSN: | 1347-5223 0009-2363 |
DOI: | 10.1248/cpb.50.1114 |
Popis: | The application of the refocused-decoupled INEPT pulse sequence in 13C-NMR spectroscopy allows, in conjonction with computer simulations, a straightforward editing of the spectra of a raw mixture of glycosidic compounds. |
Databáze: | OpenAIRE |
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