Determination of sulfanilamide based on the Mn(II)-catalyzed oscillating chemical reaction
| Autor: | Xiaoxia Wei, Jie Ren, Dong-Yu Lv, Hua Chen, Hongxia Dai, Wu Yang, Jie Qu, Jinzhang Gao |
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| Rok vydání: | 2007 |
| Předmět: |
Detection limit
Chemistry Analytical chemistry General Chemistry Sulfanilamide Chemical reaction continuous-flow stirred tank Catalysis Linear relationship sulfanilamide mn(ii)-catalysed oscillating chemical reaction analyte pulse perturbation technique Materials Chemistry medicine QD1-999 medicine.drug |
| Zdroj: | Open Chemistry, Vol 5, Iss 2, Pp 581-589 (2007) |
| ISSN: | 2391-5420 |
| DOI: | 10.2478/s11532-007-0007-y |
| Popis: | A convenient and sensitive method for determination of sulfanilamide (SNA) was described based on the Mn(II)-catalyzed oscillating chemical reaction. Under optimum conditions, a linear relationship existed between the changes of oscillating period or amplitude and the negative of logarithm of SNA concentration in the range of 4.27 × 10−8 mol ·L−1 ∼ 7.41 × 10−6 mol ·L−1 (RSD, 0.85%) and 9.33 × 10−8 mol ·L−1 ∼ 3.02 × 10−6 mol ·L−1 (RSD, 1.08%), respectively. The lower limit of detection was found to be 2.69 × 10−8 mol ·L−1 and 6.03 × 10−8 mol ·L−1, respectively. |
| Databáze: | OpenAIRE |
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