Development of a method for the determination of citrinin in barley, rye and wheat by solid phase extraction on aminopropyl columns and HPLC-FLD

Autor:	A. Hartl, W. R. Stenzel
Rok vydání:	2007
Předmět:	Detection limit Chromatography Extraction (chemistry) Ethyl acetate food and beverages Toxicology Microbiology High-performance liquid chromatography Citrinin chemistry.chemical_compound chemistry Hplc fld Solid phase extraction Mycotoxin Biotechnology
Zdroj:	Mycotoxin Research. 23:127-131
ISSN:	0178-7888
DOI:	10.1007/bf02951508
Popis:	A method for the determination of the mycotoxin citrinin (CT) in rye, wheat and barley is described. The proposed method is based on ethyl acetate extraction, solid phase clean-up (SPE) on aminopropyl columns and reversed phase high performance liquid chromatography with fluorescence detection (RP-HPLC-FLD). The limits of detection and quantification of CT amounted to 0.6-0.9 μg/kg and 1.7- 3.3 μg/kg with mean recovery rates in the range of 77-92% (RSD 4.8-5.5%). This method can also be used for the determination of CT in red-fermented rice.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::1f8b5a262ded0e35e66ddb3e79d2008f https://doi.org/10.1007/bf02951508 Zobrazit plný text záznamu Full text from SpringerLink