Chemical Etching Technique for the Investigation of Melt-crystallized Isotactic Polypropylene Spherulite and Lamellar Morphology by Scanning Electron Microscopy

Autor: Ohjun Kwon, Kyuyoung Eom, Jemyung Park, Sangsun Woo
Rok vydání: 2003
Předmět:
Zdroj: Microscopy and microanalysis : the official journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada. 7(3)
ISSN: 1435-8115
Popis: The spherulitic and lamellar morphologies of melt crystallized isotactic polypropylene (iPP) have been investigated according to various crystallization temperatures and times. In this study, an appropriate chemical etching condition for the observation of iPP morphology by scanning electron microscopy (SEM) is determined. The optimum etchant formulation is 3 wt% potassium permanganate with the mixed solvent of sulfuric acid and phosphoric acid. The morphologies after etching reveal the microstructure of iPP clearly, such as the characterization of α/β spherulites and the different lamellar growth patterns.
Databáze: OpenAIRE