Determination of triclosan in foodstuffs
| Autor: | Raquel Sendón-García, Julia López-Hernández, A. Sanches-Silva, Perfecto Paseiro-Losada |
|---|---|
| Rok vydání: | 2005 |
| Předmět: |
Meat
Food Contamination Filtration and Separation High-performance liquid chromatography Gas Chromatography-Mass Spectrometry Mass Spectrometry Analytical Chemistry Beverages chemistry.chemical_compound Cheese Animals Chromatography High Pressure Liquid Orange juice Residue (complex analysis) Chromatography Extraction (chemistry) Food Packaging Triclosan Hexane Food packaging chemistry Anti-Infective Agents Local Spectrophotometry Ultraviolet Gas chromatography–mass spectrometry Chickens Food Analysis Citrus sinensis |
| Zdroj: | Journal of Separation Science. 28:65-72 |
| ISSN: | 1615-9314 1615-9306 |
| DOI: | 10.1002/jssc.200401845 |
| Popis: | A reverse-phase high-performance liquid chromatographic (RP-HPLC) method coupled with an ultraviolet detector was developed to determine triclosan which had migrated into foodstuffs from packaging materials. The method includes extraction with hexane, followed by evaporation to dryness and residue re-dissolution in ACN 90%. Chromatographic separation was performed with a Kromasil 100 C18 column (15 cm x 0.4 cm ID, 5 microm particle size) at 30 degrees C and using ACN and water as mobile phases. Regarding recoveries, good results (higher than 83% and lower than 112%) were obtained for the three representative food matrixes selected (orange juice, chicken breast meat, and Gouda cheese). |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Plný text