Impact of growth velocity on grain structure formation during directional solidification of a refined Al-20wt.%Cu alloy

Autor: H. Soltani, M. Zahzouh, F. Ngomesse, Guillaume Reinhart, Henri Nguyen-Thi, M.C. Benoudia
Přispěvatelé: Université Badji Mokhtar - Annaba [Annaba] (UBMA), Institut des Matériaux, de Microélectronique et des Nanosciences de Provence (IM2NP), Université de Toulon (UTLN)-Centre National de la Recherche Scientifique (CNRS)-Aix Marseille Université (AMU), Ecole Nationale Supérieure des Mines et de la Métallurgie, L3M, Université Badji Mokhtar Annaba (UBMA), Aix Marseille Université (AMU)-Université de Toulon (UTLN)-Centre National de la Recherche Scientifique (CNRS), GDR 2799 Micropesanteur Fondamentale & Appliquée
Jazyk: angličtina
Rok vydání: 2020
Předmět:
Zdroj: Journal of Crystal Growth
Journal of Crystal Growth, Elsevier, 2020, 548, pp.125819. ⟨10.1016/j.jcrysgro.2020.125819⟩
Journal of Crystal Growth, 2020, 548, pp.125819. ⟨10.1016/j.jcrysgro.2020.125819⟩
ISSN: 0022-0248
DOI: 10.1016/j.jcrysgro.2020.125819⟩
Popis: The paper presents detailed analyses of solidification experiments performed on a refined Al-20 wt.%Cu alloy using the SFINX (Solidification Furnace with IN situ X-radiography) laboratory facility. Directional solidifications of a sheet-like sample were carried out in a horizontal configuration, with the main surface of the sample parallel to the ground. The sample was solidified for a wide range of cooling rates to obtain various grain structures, from columnar to elongated and equiaxed. The formation of the grain structure was observed in-situ and in real-time by X-radiography, which allows the dynamic of solidification phenomena to be thoroughly analyzed. Based on the radiographs, quantitative measurements were performed to accurately describe the solidified grain structure, namely the nucleation position, nucleation rate, grain size, grain elongation factor and growth orientation. The experiments showed that increasing the growth velocity leads to a decrease of both the grain size and grain elongation factor, resulting in a more homogeneous and isotropic grain distribution. The grain characteristic parameters were also sensitive to variations of the temperature gradient in the Field-of-View. The results were discussed by analyzing the impact of the solidification parameters on the constitutionally undercooled liquid zone ahead of the solidification front.
Databáze: OpenAIRE