Nanocharacterization of the Graphene Oxide Terminated Platform on Polycrystalline Gold Surface
| Autor: | İhsan Aşık, Haslet Ekşi, Aslıerkal, Mehmet Selçuk Erdoğan, Saadet Uluok, Gamze Kuzu, Zafer Üstündağ |
|---|---|
| Rok vydání: | 2015 |
| Předmět: |
X-ray photoelectron spectroscopy
Materials science Graphene Oxide Nanotechnology General Chemistry Nanofilm Condensed Matter Physics law.invention Computational Mathematics chemistry.chemical_compound chemistry law General Materials Science Gold surface Crystallite Electrical and Electronic Engineering Infrared spectroscopy Graphene oxide Graphene oxide paper |
| Zdroj: | Journal of Computational and Theoretical Nanoscience. 12:1787-1794 |
| ISSN: | 1546-1955 |
| Popis: | Graphene oxide phenoxyamide nanofilm (AP-GO) was covalently grafted on to polycrystalline gold platform by using cyclic voltammetry (CV). Initially, nitrophenyl (NP-) group was attached to the polycrystalline gold (Au) substrate through the electroreduction of 4-nitrobenzene diazonium salt (NB-DAS). Thereafter, nitrophenyl-modified electrode (Au-NP) was exposed to negative potential scan to reduce the nitro group to amine group (AP-). 4-Aminophenyl modified gold platform (Au-AP) was dipped into a electrochemically synthesized graphene oxide solution containing 1-ethyl-3(3-(dimethlyamino) propyl)-carbodiimide (EDC) as an activating solution. Thus formed Graphene oxide phenoxyamide modified gold substrate was denoted as Au-AP-GO. The nanoplatform was characterized by electrochemical method like cyclic voltammetry (CV) and spectroscopic techniques such as X-ray photoelectron spectroscopy (XPS) and diamond crystal accesorized attenuated total reflectance infrared spectroscopy Delivered by (ATR-FTIR). Publishing Layer Technology thickness to: of Elsevier the nanofilms BV on gold substrate was measured using an ellipsometer. Copyright © 2015 American Scientific Publishers All rights reserved. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|