Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate
| Autor: | Raúl Ricardo Díaz-Contreras, Angel Zamudio-Medina, Marco Franco-Pérez, Galdina Vanessa Suárez-Moreno, Oscar Ernesto Guevara-Moreno, José L. Castrejón-Flores, Atilano Gutiérrez-Carrillo |
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| Rok vydání: | 2019 |
| Předmět: |
010405 organic chemistry
Organic Chemistry One-pot synthesis Nuclear magnetic resonance spectroscopy 010402 general chemistry Mass spectrometry 01 natural sciences Biochemistry Phosphonate Combinatorial chemistry 0104 chemical sciences Catalysis Inorganic Chemistry Diethyl chlorophosphate chemistry.chemical_compound chemistry Imidazole |
| DOI: | 10.6084/m9.figshare.8019413.v1 |
| Popis: | We present a multicomponent reaction strategy to synthesize a (dihydro-1H-benzo[d]imidazole)phosphonate family of compounds, using benzimidazoles, diethyl chlorophosphate and aliphatic amines as starting reactants. Giving its simplicity, our procedure involves reaction times of only few hours and avoid the usage of any catalyst agent. All the newly synthesized compounds were characterized by Nuclear Magnetic Resonance spectroscopy (1H, 13C and 31P) and mass spectrometry by the DART method. |
| Databáze: | OpenAIRE |
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