| Autor: |
Wurzer, Alexander, Carlo, Daniel Di, Herz, Michael, Richter, Antonia, Robu, Stephanie, Schirrmacher, Ralf, Mascarin, Alba, Weber, Wolfgang, Eiber, Matthias, Schwaiger, Markus, Hans-Juergen Wester |
| Rok vydání: |
2021 |
| DOI: |
10.6084/m9.figshare.13634500 |
| Popis: |
Additional file 1: Supplemental Figure 1. Exemplary HPLC chromatogram (Radioactivity and UV) of the formulated product [18F]Ga-rhPSMA-7.3. The peak at retention time 6.7 min (radioactivity-channel) and 6.4 min (UV-channel) corresponds to [18F]Ga-rhPSMA-7.3. HPLC analysis was performed on a Prominence system, equipped with a variable wavelength detector (both Shimadzu) and a gamma-detector Gabi Star (Elysia-raytest). Water/0.1% TFA (solvent A) and MeCN (solvent B) served as mobile phases, a Nucleosil 100-5 C18 column of 125×4 mm was used as stationary phase. For sample analysis, 10 μL of product solution were injected and the following linear solvent gradient was applied: 30-38% B in 9 min, 38-95% B in 8 min, back to 30% B in 1 min and re-equilibration at 30% B for 1.5 min (flowrate = 1 mL/min, at 240 nm). |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
|
