| Autor: |
Carolina Belenguer-Sapiña, Enric Pellicer-Castell, Jamal El Haskouri, Ernesto Francisco Simó-Alfonso, Pedro Amorós, Adela R. Mauri-Aucejo |
| Rok vydání: |
2022 |
| Předmět: |
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| Zdroj: |
Food Chemistry. 380:132207 |
| ISSN: |
0308-8146 |
| DOI: |
10.1016/j.foodchem.2022.132207 |
| Popis: |
An innovative material based in type UVM-7 mesoporous silica containing analyte-accessible cyclodextrin units is described and assessed as a selectivity-enhancing sorbent for extracting endocrine-disrupting chemicals from bottled apple juice to subsequently quantify them. The synthesis procedure has been carried out using both β- and γ-cyclodextrin for their later comparison. Then, a complete analytical method for the isolation and determination of the above analytes has been validated. Following the optimized procedure, recoveries between 94% and 100% have been achieved and good repeatability is obtained with deviations under 6.8% for intra-day and inter-day experiments. The detection limits of the method have been established in the ng L |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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