Qualitative TLC determination of some polycyclic aromatic hydrocarbons in sugar-beet
| Autor: | Eva S. Lončar, Biljana Škrbić, Radomir V. Malbaša, Ljiljana A. Kolarov |
|---|---|
| Jazyk: | angličtina |
| Rok vydání: | 2005 |
| Předmět: |
Fluoranthene
Anthracene Chromatography biology pahs Silica gel Extraction (chemistry) silica gel tlc General Chemistry biology.organism_classification Thin-layer chromatography cyclohexane extracts lcsh:Chemistry chemistry.chemical_compound chemistry lcsh:QD1-999 sugar-beet Pyrene Sugar beet Saponification |
| Zdroj: | Journal of the Serbian Chemical Society, Vol 70, Iss 10, Pp 1237-1242 (2005) |
| ISSN: | 1820-7421 0352-5139 |
| Popis: | The presence of polycyclic or polynuclear aromatic hydrocarbons (PAHs) were investigated in sugar-beet from a local sugar factory in the district of Vojvodina. The sugar-beet was cultivated on areas near roads with intensive traffic. The procedure for the preparation and determination of these compounds included saponification of the sample, several liquid?liquid extraction systems and a silica gel column clean-up. The purified sample solution was analysed by thin layer chromatography (TLC) on silica gel with cyclohexane as the developing solvent. Benzo(b)fluoranthene and benzo(a)anthracene and/or benzo(a)pyrene were detected at concentrations greater than the allowed limits in food. |
| Databáze: | OpenAIRE |
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