Quaternary ferrites by batch and continuous flow hydrothermal synthesis: a comparison
| Autor: | Paolo Pastore, Charles J. M. Footer, Nicola Dengo, Silvia Gross, Michele Bastianello, Jawwad A. Darr, Stefano Diodati, Denis Badocco, Liam McCafferty |
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| Rok vydání: | 2019 |
| Předmět: |
Materials science
Continuous flow Spinel 02 engineering and technology General Chemistry engineering.material 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences 0104 chemical sciences Chemical engineering X-ray photoelectron spectroscopy CHFS engineering Hydrothermal synthesis General Materials Science 0210 nano-technology |
| Zdroj: | CrystEngComm. 21:6801-6809 |
| ISSN: | 1466-8033 |
| DOI: | 10.1039/c9ce01462d |
| Popis: | Crystalline spinel quaternary ferrites MxZn1−xFe2O4 (M = Co, Ni; x = 0.2, 0.35, 0.5, 0.65, 0.8) were synthesised through conventional batch hydrothermal synthesis (HT) at 135 °C as well as via continuous flow hydrothermal synthesis (CHFS). The as prepared compounds were thoroughly characterised from a compositional (ICP-MS, XPS) and structural (XRD) point of view in order to compare the synthetic approaches and achieve a greater understanding of how the chosen approach influences the characteristics of the resulting spinel. |
| Databáze: | OpenAIRE |
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