Hydrophosphorylation of vinyl sulfides with elemental phosphorus in the KOH/DMSO(H2O) system: synthesis of 2-alkyl(aryl)thioethylphosphinic acids

Autor:	B. A. Trofimov, A. V. Artem’ev, N. K. Gusarova, A. O. Sutyrina, S. F. Malysheva, L. A. Oparina
Rok vydání:	2017
DOI:	10.6084/m9.figshare.5572603.v1
Popis:	Elemental phosphorus (red or white) reacts with alkyl and aryl vinyl sulfides in the superbase system KOH/DMSO(H2O) at 75–120°C for 2–3 h to afford 2-alkyl(aryl)thioethylphosphinic acids in a yield of up to 31%.
Databáze:	OpenAIRE
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