Supercritical extraction of solid materials: a practical correlation related with process scaling
| Autor: | Tiziana Fornari, Guillermo Reglero, Alejandro Ruiz-Rodríguez, Alexis López-Padilla |
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| Přispěvatelé: | UAM. Departamento de Química Física Aplicada, Comunidad de Madrid, Colciencias (Colombia), Agencia de Educación Superior de Medellín |
| Rok vydání: | 2017 |
| Předmět: |
Work (thermodynamics)
Materials science 02 engineering and technology Raw material 01 natural sciences Supercritical fluid extraction Barton model Mass transfer Porosity Process engineering Scaling Scaling up business.industry 010401 analytical chemistry Extraction (chemistry) Química 021001 nanoscience & nanotechnology 0104 chemical sciences Overall extraction curve Particle 0210 nano-technology business Food Science |
| Zdroj: | Biblos-e Archivo. Repositorio Institucional de la UAM Consejo Superior de Investigaciones Científicas (CSIC) Biblos-e Archivo: Repositorio Institucional de la UAM Universidad Autónoma de Madrid Digital.CSIC. Repositorio Institucional del CSIC instname |
| Popis: | The supercritical fluid extraction (SFE) of vegetal raw materials is a large field of research, innovation and entrepreneurial developments. Optimization of process conditions is usually accomplished in analytical or laboratory scale equipment. Although SFE scaling is essential to attain industrial applications, studies in the literature are scarce. In this work, the kinetic behavior of 19 overall extraction curves (OEC’s), obtained by the authors in previous works using NOVALINDUS Platform SFE facilities, and a set of 39 OEC’s published by other authors, were considered all together to study SFE scaling. A general trend between the solvent flow rate and Barton kinetic constant was obtained for all extraction curves included in the data base, which comprise 10 different plant materials, temperatures in the range 298–333 K, pressures of 10–30 MPa, extractor volumes from 50 to 5200 cm3, particle diameters from 250 to 1400 μm and bed porosity in the range 0.59–0.97. López-Padilla A. Thanks to COLCIENCIAS (568–2012) and Medellin Mayor’s Office (Sapiencia/Enlaza Mundos Program, 2013) for the Ph.D. fellowship. This work was financed thanks ALIBIRD, S2013/ABI-2728 (Comunidad de Madrid) project. |
| Databáze: | OpenAIRE |
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