Synthesis and structural characterization of a novel amine-bis(phenolate)ligand

Autor:	Laura Rodríguez-Silva, Sandra Fernández-Fariña, M. I. Romero, Esther Gómez-Fórneas, Luis M. González-Barcia, Maria Isabel Fernandez-Garcia
Rok vydání:	2017
Předmět:	chemistry.chemical_classification chemistry.chemical_compound Chemistry Ligand Tripodal ligand Polymer chemistry Formaldehyde Phenol Amine gas treating Carbon-13 NMR Organic compound Mannich reaction
Zdroj:	Proceedings of The 21st International Electronic Conference on Synthetic Organic Chemistry.
DOI:	10.3390/ecsoc-21-04774
Popis:	The substituted amine-bis(phenol) compound N,N-bis-(4,5-dimethyl-2-hydroxybenzyl)-N(2-pyridylethyl)amine (H2L) was prepared through a Mannich reaction utilizing two equivalents of a substituted phenol, two equivalents of formaldehyde and a single equivalent of a secondary amine. The organic compound, which may act as a tripodal ligand in coordination complexes, has been characterized by elemental analysis, IR, and 1H and 13C NMR spectroscopies, mass spectrometry (ES) and X ray diffraction spectroscopy.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::fb5636f91b081bd87aeb589d5ddead50 https://doi.org/10.3390/ecsoc-21-04774 Zobrazit plný text záznamu