18,20-Lactone of 3β-Acetoxy-20β-Hydroxy-5-Pregnene-18-Oic Acid

Autor: Ch. Meystre, K. Heusler, P. Wieland
Rok vydání: 2003
Předmět:
Zdroj: Organic Syntheses
Popis: 18,20-Lactone of 3β-acetoxy-20β-hydroxy-5-pregnene-18-oic acid intermediate: 3β-Acetoxy-20β-hydroxy-5-pregnene reactant: 71.7 g. (0.2 mole) of pregnenolone acetate intermediate: 3β-Acetoxy-18-iodo- and 18-hydroxy-18,20β-oxido-5-pregnene product: 18,20-lactone of 3β-acetoxy-20β-hydroxy-5-pregnene-18-oic acid Keywords: annulation, heterocyclic-[5]; cyclization, oxidative cyclization; reduction, CO CHOH; tetrahydrofuran, removal of peroxides
Databáze: OpenAIRE