An effective precursor for growth of bubble-chain boron nitride nanotubes
Autor: | Zhan Hui Zhang, Yunle Gu, Laiping Zhang, Guo Wei Zhao, Xinye Pan, Jilin Wang |
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Rok vydání: | 2013 |
Předmět: |
Materials science
Annealing (metallurgy) Biomedical Engineering Bioengineering Amorphous solid Optical properties of carbon nanotubes Condensed Matter::Materials Science chemistry.chemical_compound symbols.namesake Crystallography chemistry Chemical engineering Boron nitride symbols General Materials Science Fourier transform infrared spectroscopy Raman spectroscopy High-resolution transmission electron microscopy Powder diffraction |
Zdroj: | Journal of Experimental Nanoscience. 8:833-841 |
ISSN: | 1745-8099 1745-8080 |
Popis: | Large amounts of bubble-chain boron nitride nanotubes were synthesised by annealing an effective precursor. The porous precursor was produced by self-propagation high-temperature synthesis method using Mg, B2O3, amorphous B and Fe2O3 as the starting materials, which played an important role in synthesis of BN nanotubes in large quantities. Samples were characterised by SEM, TEM, HRTEM, X-ray powder diffraction and Raman and Fourier transform infrared spectroscopy. The as-synthesised BN nanotubes revealed periodical bubble-chain structures, having diameters of range 20–200 nm and an average length of more than 5 µm. The effects of temperature, time and the possible mechanism of the growth of the BN nanotubes were also discussed. |
Databáze: | OpenAIRE |
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