Soft X-Ray Microscopic Investigation on Self Assembling Nanocrystals

Autor: M. Benk, K. Bergmann, A. Querejeta-Fernández, S. Srivastava, N. A. Kotov, D. Schaefer, T. Wilhein, Ian McNulty, Catherine Eyberger, Barry Lai
Rok vydání: 2011
Předmět:
Zdroj: AIP Conference Proceedings.
ISSN: 0094-243X
DOI: 10.1063/1.3625395
Popis: Soft x‐ray microscopy is well suited to investigation of nanoparticles in liquid media. Using a table‐top microscope based on a gas‐discharge source emitting at 2.88 nm, dried CdTe nanowires and dried PbS hyperbranched nanocrystals are investigated. These structures are the result of the assembly of nanoparticles in a liquid environment. Soft x‐ray microscopy is aiming at a better understanding of underlying parameters that affect the self assembly to the desired final structures. It is shown that the presented setup is able to image these particles with a resolution of about 50 nm with exposure times in the range of tens of seconds. The discharge source has a photon flux of more than 109 photons/(sr s μm2) at a photon energy of 430 eV with a bandwidth of λ/Δλ = 840. The repetition rate of the source is up to 1000 Hz. With the current setup a photon flux of 5×106 photons/(μm2 s) at the sample is achieved.
Databáze: OpenAIRE